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刊物期号: 201811

竹叶青酒中橙皮苷含量的测定方法研究(106)

作者: 崔 帆,杨凯环,李晓晓,李素琴,吴成斌,任 杰

地址:山西杏花村汾酒厂股份有限公司技术中心,山西 汾阳 邮编:032205
摘要 通过比较在3种色谱条件下测定竹叶青酒中橙皮苷含量的情况,选择一种最适合应用于我公司的测定方法。采用ACQUITY UPLC H-CLASS,BEH C18色谱柱(1.7 μm,2.1×50 mm)及Waters e2695型高效液相色谱仪,Symmetry C18柱(250 mm×4.6 mm,5 μm)两个仪器的3种色谱条件进行了测定。结果表明,3种条件下橙皮苷进样量在0.0021~0.252 mg/mL范围内与峰面积线性良好。橙皮苷的平均回收率分别为94.74 %、94.63 %、94.60 %,相对标准偏差(RSD)分别为1.7 %、1.4 %、1.78 %。经过综合比较,方法二成本低,出峰时间较快,回收率好,误差较小,所以考虑选择方法二测定竹叶青酒中的橙皮苷含量。
关键词 竹叶青酒; 橙皮苷; 超高效液相色谱法; 高效液相色谱法; 含量测定
中图分类号: TS262.91;TS261.4;TS261.7 文献标识码: A 文章编号: 1001-9286(2018)11-0106-04

英文标题: Determination of Hesperidin Content in Zhuyeqing Liquor

英文作者: CUI Fan, YANG Kaihuan, LI Xiaoxiao, LI Suqin, WU Chengbin and REN Jie

英文地址: Technical Center of Xinghuacun Fenjiu Distillery Co. Ltd., Fenyang, Shanxi 032205, China

英文摘要 Through the comparison of the determination of hesperidin content in Zhuyeqing Liquor under three different chromatographic conditions (ACQUITY UPLC H-CLASS, BEH C18 column (1.7 μm, 2.1×50 mm), and HPLC with Symmetry C18 column (250 mm×4.6 mm, 5 μm)), the results showed that, within the range of 0.0021 mg/mL to 0.252 mg/mL, hesperidin had a good liner relation to the peak area under these three conditions; the average recovery rate of hesperidin were 94.74 %, 94.63 % and 94.60 % respectively, and RSD were 1.7 %, 1.4 % and 1.78 % respectively. The comparison suggested that BEH C18 column (1.7 μm, 2.1×50 mm) had the advantages including low cost, fast peak time, good recovery rate and small error. Accordingly, it was selected as the determination method of hesperidin content in Zhuyeqing liquor in our distillery.
英文关键词 Zhuyeqing Liquor; hesperidin; UPLC; HPLC; content determination
      

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